Synthesis, characterization, crystallization kinetics of amorphous Fe74.5Zr8.5B17 magnetic nanoparticles, and magnetoelectric properties of Fe74.5Zr8.5B17/BaTiO3 composite
Journal of Materials Science: Materials in Electronics, cilt.36, sa.2, 2025 (SCI-Expanded, Scopus)
- Yayın Türü: Makale / Tam Makale
- Cilt numarası: 36 Sayı: 2
- Basım Tarihi: 2025
- Doi Numarası: 10.1007/s10854-024-14186-9
- Dergi Adı: Journal of Materials Science: Materials in Electronics
- Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Aerospace Database, Applied Science & Technology Source, Chemical Abstracts Core, Communication Abstracts, Compendex, Computer & Applied Sciences, INSPEC, MEDLINE, Metadex, Civil Engineering Abstracts
- Açık Arşiv Koleksiyonu: AVESİS Açık Erişim Koleksiyonu
- İnönü Üniversitesi Adresli: Evet
Özet
This work reports the facile synthesis of amorphous Fe74.5 Zr8.5 B17 magnetic nanoparticles (MNPs) through a simple NaBH4-assisted chemical reduction method. The obtained MNPs were characterized in terms of amorphous/crystal structure, morphology, magnetic properties, composition, and crystallization kinetics. The saturation magnetization value was determined as 57.83 emu/g. The crystallization peak temperatures (Tp) and activation energy were determined to be 467.18 °C and 294 kJ/mol, respectively. Additionally, the FeZrB MNPs were combined with the BaTiO3 NPs via ball milling at low speed, using a mass ratio of 30/70%, respectively and the magnetoelectric coefficient value for FeZrB/BaTiO3 composite measured at a 1 kHz AC magnetic field is approximately 8.9 mV/Oe/cm. The study outcomes may provide a platform of nanotechnology for the preparation of MNPs with adjustable properties, which will be promising for practical applications.